HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylisoquinoline-5-sulfonyl chloride → HCID 22121916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylisoquinoline-5-sulfonyl chloride | HCID 15487110 | — |
| Reactant | 1,1-Dimethylethyl 3-ethylhexahydro-1H-1,4-diazepine-1-carboxylate | HCID 22121891 | — |
| Product | HCID 22121916 | HCID 22121916 | 34.5% |
Reaction Steps
Using 0.68 g of 1-(tert-butoxycarbonyl)-3-ethyl-hexahydro-1H-1,4-diazepine and 0.72 g of 5-chlorosulfonyl-4-methylisoquinoline, the procedure of Example 1 was otherwise repeated to provide 0.38 g of the objective compound (white crystals).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06153608 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-61d1178f408d48f3954b6546e4942c8b |
| Source note | uspto-grants-2000_11 |