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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1858942Erstellt: 26. Oktober 2026

Potassium Carbonate → 1-[4-(1,3-Benzodioxol-5-yl)-3-cyclohexen-1-yl]-4-[(2-chlorophenyl)methyl]piperazine

https://huagongshe.com/reaction/1858942

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium CarbonateHCID 11430—
Edukt2-Chlorobenzyl chlorideHCID 11906—
Edukt1-[4-(1,3-Benzodioxol-5-yl)-3-cyclohexen-1-yl]piperazineHCID 22122062—
Produkt1-[4-(1,3-Benzodioxol-5-yl)-3-cyclohexen-1-yl]-4-[(2-chlorophenyl)methyl]piperazineHCID 22122065—

Reaktionsschritte

The title compound was prepared from 2-chlorobenzyl-chloride (0.16 g, 1 mmole), 1-[4-(1,3-benzodioxol-5-yl)-3-cyclohexen-1-yl]piperazine (0.29 g, 1 mmole), and excess powdered K2CO3 as described in example 45 to give the product (78%, mp: 115-116° C.). Calc'd for C24H27ClN2O2 : C, 70.14%; H, 6.62%; N, 6.82%. Found: C, 70.25; H, 6.69%; N, 6.83%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06153611
Quelldatensatzuspto-grants-2000_11
ORD IDord-b4934d3b67474201b20d5f37cfd3c2c5
Quellennotizuspto-grants-2000_11