HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → 1-[4-(1,3-Benzodioxol-5-yl)-3-cyclohexen-1-yl]-4-[(2-chlorophenyl)methyl]piperazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 2-Chlorobenzyl chloride | HCID 11906 | — |
| Edukt | 1-[4-(1,3-Benzodioxol-5-yl)-3-cyclohexen-1-yl]piperazine | HCID 22122062 | — |
| Produkt | 1-[4-(1,3-Benzodioxol-5-yl)-3-cyclohexen-1-yl]-4-[(2-chlorophenyl)methyl]piperazine | HCID 22122065 | — |
Reaktionsschritte
The title compound was prepared from 2-chlorobenzyl-chloride (0.16 g, 1 mmole), 1-[4-(1,3-benzodioxol-5-yl)-3-cyclohexen-1-yl]piperazine (0.29 g, 1 mmole), and excess powdered K2CO3 as described in example 45 to give the product (78%, mp: 115-116° C.). Calc'd for C24H27ClN2O2 : C, 70.14%; H, 6.62%; N, 6.82%. Found: C, 70.25; H, 6.69%; N, 6.83%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06153611 |
| Quelldatensatz | uspto-grants-2000_11 |
| ORD ID | ord-b4934d3b67474201b20d5f37cfd3c2c5 |
| Quellennotiz | uspto-grants-2000_11 |