Potassium Carbonate → 1-[4-(1,3-Benzodioxol-5-yl)-3-cyclohexen-1-yl]-4-[(3-methoxyphenyl)methyl]piperazine

Participants

Reaction Steps

The title compound was prepared from 3-methoxybenzyl chloride (0.13 g, 0.8 mmole), 1-[4-(1,3-benzodioxol-5-yl)-3-cyclohexen-1-yl]piperazine (0.23 g, 0.8 mmole), and excess powdered K2CO3 as described in example 45 to give the product (45%, mp: 124-124.5° C.). Calc'd for C25H30N2O3 : C, 73.86%; H, 7.44%; N, 6.89%. Found: C, 73.88; H, 7.43%; N, 6.91%.

Provenance & Evidence