HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 11414429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 86756067 | HCID 86756067 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 11414429 | HCID 11414429 | 96.7% |
Reaction Steps
A solution of 4 g of compound obtained in Step C in 50 ml of tetrahydrofuran is added dropwise to a suspension of 1.03 g of LiAlH4 in 15 ml of tetrahydrofuran. The mixture is left overnight at ambient temperature. After hydrolysis and filtering off the salts, evaporation to dryness is carried out to obtain 3.5 g of expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06153640 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-f82a6ba682ed4fa7813f29982d7a80e5 |
| Source note | uspto-grants-2000_11 |