HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 86756069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 86756070 | HCID 86756070 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86756069 | HCID 86756069 | — |
Reaction Steps
3.32 g of the product obtained in Step C are introduced, in portions, into a suspension composed of 0.73 g of lithium aluminium hydride and 53 ml of tetrahydrofuran. After 2 hours at ambient temperature, the medium is hydrolysed in the cold state and the precipitate formed is filtered off. After evaporating off the solvent, the expected product is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06153640 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-815f1672dee14c5dad411a051ac53e2c |
| Source note | uspto-grants-2000_11 |