HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 22123263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 22123300 | HCID 22123300 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22123263 | HCID 22123263 | — |
Reaction Steps
The product from step b) was heated with ammonium hydroxide (5 mL) and dimethylformamide (5 mL) at 75° C. for 5 h in a sealed flask. The flask was cooled and the content partitioned between ethyl acetate and water. The organic phase was washed with ammonium hydroxide. Evaporation afforded 188 mg of the sub-title product, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06153641 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-08eb542c40114b818594b98da8549975 |
| Source note | uspto-grants-2000_11 |