Sulfuric Acid → HCID 18625151, compound

HRID 1859368Notes

Reaction equation

HRID 1859368 reaction equation
[C:1]([N:10]([CH3:16])[CH2:11][CH2:12][C:13]([OH:15])=[O:14])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(=O)(=O)(O)O.[CH:22](O)([CH3:24])[CH3:23]>>[CH:22]([O:14][C:13](=[O:15])[CH2:12][CH2:11][N:10]([C:1](=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])[CH3:16])([CH3:24])[CH3:23]

Participants

4

Reactant 3

HCID 1118Sulfuric AcidHCID 3776IsopropanolHCID 18625149Capryloyl methyl beta-alanine

Product 1

HCID 18625151HCID 18625151, compound

Procedure

Fifty-seven(57) grams of N-octanoyl-N-methyl-β-alanine and 500 ml of isopropanol were charged into a 1,000-milliliter flask, and 1 ml of conc. sulfuric acid was further added thereto as the catalyst. The mixture was heated under reflux reaction for 8 hours.

Workup

  1. temperatureThe mixture was heated
  2. temperatureunder reflux
  3. customreaction for 8 hours

Sources & evidence

ORD record
ord-8bcbfa809426476db72b76e486fe6dd5
Source dataset
uspto-grants-2003_03
Patent number
US06528068B1

Reaction notes

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