Sulfuric Acid → HCID 18625136, compound

HRID 1859369Notes

Reaction equation

HRID 1859369 reaction equation
[C:1]([N:14]([CH3:20])[CH2:15][CH2:16][C:17]([OH:19])=[O:18])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].S(=O)(=O)(O)O.[CH:26](O)([CH3:28])[CH3:27]>>[CH:26]([O:18][C:17](=[O:19])[CH2:16][CH2:15][N:14]([C:1](=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:20])([CH3:28])[CH3:27]

Participants

4

Procedure

One hundred grams(100) of N-lauroyl-N-methyl-β-alanine and 750 ml of isopropanol were charged into a 1,000-milliliter flask. Further, 2 ml of conc. sulfuric acid were added as the catalyst. The mixture was heated under ref lux for reaction for 8 hours.

Workup

  1. temperatureThe mixture was heated under ref lux for reaction for 8 hours

Sources & evidence

ORD record
ord-3996145788194df08bb625b2f0a17974
Source dataset
uspto-grants-2003_03
Patent number
US06528068B1

Reaction notes

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