Sulfuric Acid → HCID 18625148, compound

HRID 1859371Notes

Reaction equation

HRID 1859371 reaction equation
[C:1]([N:14]([CH2:16][C:17]([OH:19])=[O:18])[CH3:15])(=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].S(=O)(=O)(O)O>C(O)CCC>[CH2:1]([O:18][C:17](=[O:19])[CH2:16][N:14]([C:1](=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:15])[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 1118Sulfuric AcidHCID 7348Lauroylsarcosine

Product 1

HCID 18625148HCID 18625148, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

One hundred and thirty-five point five(135.5) grams of N-lauroylsarcosine (ex. Kawaken Fine Chemicals Co., Ltd.) and 200 ml of 1-butanol were charged into a 500-milliliter flask. Further, 4.99 g of conc. sulfuric acid were added as the catalyst. The mixture was heated under reflux for reaction for 6 hours.

Workup

  1. temperatureThe mixture was heated
  2. temperatureunder reflux for reaction for 6 hours

Sources & evidence

ORD record
ord-4c0b174462974ac89e2b7c1c36a908e1
Source dataset
uspto-grants-2003_03
Patent number
US06528068B1

Reaction notes

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