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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1859442Generated: November 1, 2026

HCID 12018620, compound → HCID 69900681, compound

https://huagongshe.com/reaction/1859442

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 12018620HCID 12018620—
ReactantHydrogen chloride-ethyl acetateHCID 21866389—
SolventDichloromethaneHCID 6344—
ProductHCID 69900681HCID 69900681—

Reaction Steps

1.5 ml of 4 M hydrochloric acid/ethyl acetate was added to a solution of (R)-5,11-dihydro-5-[1-(4-dimethylaminophenethyl)piperidine-2-ylmethyl]dibenzo[b,e][1,4]oxazepine (171 mg) in dichloromethane (5 ml), and they were stirred for 2 hours. The solvent was evaporated under reduced pressure. The title compound was obtained in the form of a light yellow solid (220 mg, 84%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06528504B2
Source datasetuspto-grants-2003_03
ORD IDord-39eccaef845d4b20906fc0ced3771b4a
Source noteuspto-grants-2003_03