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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1859462Generated: November 1, 2026

Ether hydrochloride → HCID 69897907, compound

https://huagongshe.com/reaction/1859462

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEther hydrochlorideHCID 10953452—
ReactantHCID 12018623HCID 12018623—
SolventDichloromethaneHCID 6344—
ProductHCID 69897907HCID 69897907—

Reaction Steps

3.0 ml of 2 M hydrochloric acid/ethyl ether was added to a solution of (R)-5,11-dihydro-5-[1-(3,4-methylenedioxyphenethyl) pyrrolidine-3-yl]dibenzo[b,e][1,4]oxazepine (63 mg, 0.15 mmol) in dichloromethane, and they were stirred for 1 hour. The solvent was evaporated under reduced pressure to obtain the title compound in the form of a white solid (62 mg, 91%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06528504B2
Source datasetuspto-grants-2003_03
ORD IDord-20bd492126b84c969872fbd6155bb136
Source noteuspto-grants-2003_03