HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ether hydrochloride → HCID 69897907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ether hydrochloride | HCID 10953452 | — |
| Reactant | HCID 12018623 | HCID 12018623 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69897907 | HCID 69897907 | — |
Reaction Steps
3.0 ml of 2 M hydrochloric acid/ethyl ether was added to a solution of (R)-5,11-dihydro-5-[1-(3,4-methylenedioxyphenethyl) pyrrolidine-3-yl]dibenzo[b,e][1,4]oxazepine (63 mg, 0.15 mmol) in dichloromethane, and they were stirred for 1 hour. The solvent was evaporated under reduced pressure to obtain the title compound in the form of a white solid (62 mg, 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528504B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-20bd492126b84c969872fbd6155bb136 |
| Source note | uspto-grants-2003_03 |