Ether hydrochloride → HCID 69898193, compound

HRID 1859475Notes

Reaction equation

HRID 1859475 reaction equation
[ClH:1].C(OCC)C.[CH2:7]1[O:36][C:35]2[CH:34]=[CH:33][C:11]([CH2:12][CH2:13][N:14]([CH2:16][CH2:17][N:18]3[C:24]4[CH:25]=[CH:26][CH:27]=[CH:28][C:23]=4[CH2:22][O:21][C:20]4[CH:29]=[CH:30][CH:31]=[CH:32][C:19]3=4)[CH3:15])=[CH:10][C:9]=2[O:8]1>>[ClH:1].[CH3:15][N:14]([CH2:16][CH2:17][N:18]1[C:24]2[CH:25]=[CH:26][CH:27]=[CH:28][C:23]=2[CH2:22][O:21][C:20]2[CH:29]=[CH:30][CH:31]=[CH:32][C:19]1=2)[CH2:13][CH2:12][C:11]1[CH:33]=[CH:34][C:35]2[O:36][CH2:7][O:8][C:9]=2[CH:10]=1

Participants

3

Reactant 2

HCID 10953452Ether hydrochlorideHCID 22975061HCID 22975061, compound

Product 1

HCID 69898193HCID 69898193, compound

Procedure

5 ml of 2 M hydrochloric acid/ethyl ether was added to 5,11-dihydro-5-[2-[N-(3,4-methylenedioxyphenethyl)-N-methylamino]ethyl]dibenzo[b,e][1,4]oxazepine (282 mg, 0.70 mmol), and they were stirred for 1 hour. The solvent was evaporated under reduced pressure to obtain the title compound in the form of a yellow solid (246 mg, 80%).

Workup

  1. customThe solvent was evaporated under reduced pressure

Sources & evidence

ORD record
ord-67dca5a90708483ba7a2b1d6ba85cc90
Source dataset
uspto-grants-2003_03
Patent number
US06528504B2

Reaction notes

Loading…