HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ether hydrochloride → HCID 69898193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ether hydrochloride | HCID 10953452 | — |
| Reactant | HCID 22975061 | HCID 22975061 | — |
| Product | HCID 69898193 | HCID 69898193 | — |
Reaction Steps
5 ml of 2 M hydrochloric acid/ethyl ether was added to 5,11-dihydro-5-[2-[N-(3,4-methylenedioxyphenethyl)-N-methylamino]ethyl]dibenzo[b,e][1,4]oxazepine (282 mg, 0.70 mmol), and they were stirred for 1 hour. The solvent was evaporated under reduced pressure to obtain the title compound in the form of a yellow solid (246 mg, 80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528504B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-67dca5a90708483ba7a2b1d6ba85cc90 |
| Source note | uspto-grants-2003_03 |