HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ether hydrochloride → HCID 18625625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ether hydrochloride | HCID 10953452 | — |
| Reactant | HCID 18625580 | HCID 18625580 | — |
| Product | HCID 18625625 | HCID 18625625 | — |
Reaction Steps
5 ml of 2 M hydrochloric acid/ethyl ether was added to 5,11-dihydro-5-[2-[N-(3-dimethylaminophenethyl)-N-methylamino]ethyl]dibenzo[b,e][1,4]oxazepine (296 mg, 0.74 mmol), and they were stirred for 1 hour. The solvent was evaporated under reduced pressure to obtain the title compound in the form of light green crystals (285 mg, 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528504B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-8130328ddefc465eb9dae0456438139a |
| Source note | uspto-grants-2003_03 |