Furfural → 1-Furan-2-yl 4-methyl-pent-1-en-3-one

HRID 1859515Notes

Reaction equation

HRID 1859515 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=O.[CH3:8][CH:9]([C:11](=[O:13])[CH3:12])[CH3:10]>CCO>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]=[CH:12][C:11](=[O:13])[CH:9]([CH3:10])[CH3:8]

Participants

4

Reactant 2

HCID 7362FurfuralHCID 112513-Methyl-2-butanone

Product 1

HCID 572978121-Furan-2-yl 4-methyl-pent-1-en-3-one

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The titled compound was prepared according to General Method 2 by reacting 2-furaldehyde (117 mmol), 2-methyl-butan-3-one (117 mmol), anhydrous Ba(OH)2 (2.2 g) and EtOH (200 mL) to afford the desire compound.

Workup

  1. customto afford the desire compound

Sources & evidence

ORD record
ord-ddad2e4b1608409585fb1a9cea17e8aa
Source dataset
uspto-grants-2003_03
Patent number
US06528510B1

Reaction notes

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