HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Toluene-4-thiosulfonic acid S-(4,5-diamino-2-tert-butyl-phenyl) Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | toluene-4-thiosulfonic acid S-(4,5-bis-tert-butoxycarbonylamino-2-tert-butyl-phenyl)ester | HCID 69756247 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Toluene-4-thiosulfonic acid S-(4,5-diamino-2-tert-butyl-phenyl) Ester | HCID 54523728 | — |
Reaction Steps
The title compound was prepared as described in Example VV-1 from toluene-4-thiosulfonic acid S-(4,5-bis-tert-butoxycarbonylamino-2-tert-butyl-phenyl) ester (prepared in Example UU-2; 15 g, 28 mmol), CH2Cl2 (100 mL), and HCl gas. MS(APCI): 351 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528510B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-4e9aecc5e52f4832b62e2bc918762bde |
| Source note | uspto-grants-2003_03 |