HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 5007546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | N-(4-fluoro-3-nitrophenyl)benzamide | HCID 3535228 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 5007546 | HCID 5007546 | — |
Reaction Steps
Prepared according to the procedure described for Example 10, Step A from N-(4-fluoro-3-nitrophenyl)-benzamide (5.2 g, 20 mmol) and sodium (1.3 g, 57 mmol) using methanol in place of ethanol to afford the product (3.7 g) after chromatography on silica gel in dichloromethane/methanol 99:1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-dbdec0f924e8468ea3c57b76755362e2 |
| Source note | uspto-grants-2003_03 |