HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 5007546, compound → HCID 18626083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 5007546 | HCID 5007546 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | HCID 18626083 | HCID 18626083 | 76.4% |
Reaction Steps
Prepared according to the procedure described for Example 9, Step B using N-(4-methoxy-3-nitrophenyl)-benzamide (3.68 g, 13.5 mmol) and zinc dust (20 g) to give the product (2.5 g) after chromatography on silica gel in ethyl acetate/hexane and recrystallization from the same solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-a49e96ab52e3417cb58a2eb54bd2cf8d |
| Source note | uspto-grants-2003_03 |