HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 18626251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 18626122 | HCID 18626122 | — |
| Product | HCID 18626251 | HCID 18626251 | 78.3% |
Reaction Steps
Prepared according to the procedure of Example 1 using 3-phenoxy-4-methoxybenzoic acid (0.3 g, 1.2 mmol), oxalyl chloride (0.19 g, 1.5 mmol), and aniline (0.22 g, 2.4 mmol) to afford the product (0.3 g); m.p. 200-201° C. after recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-aba36ec6eb8148c1b3f7f037ce310652 |
| Source note | uspto-grants-2003_03 |