3-Amino-4-methoxybenzanilide → HCID 53728863, compound

HRID 1859688Notes

Reaction equation

HRID 1859688 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][C:16]=1[O:17][CH3:18])[C:5]([NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:6].[C:19]([N:27]=[C:28]=[S:29])(=[O:26])[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[CH3:18][O:17][C:16]1[CH:15]=[CH:14][C:4]([C:5]([NH:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:6])=[CH:3][C:2]=1[NH:1][C:28]([NH:27][C:19](=[O:26])[C:20]1[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=1)=[S:29]

Participants

3

Reactant 2

HCID 84263-Amino-4-methoxybenzanilideHCID 68284Benzoyl isothiocyanate

Product 1

HCID 53728863HCID 53728863, compoundYield 91.5%

Procedure

Prepared according to the procedure described for Example 60 using 3-amino-4-methoxy-N-phenyl-benzamide (0.243 g, 1.0 mmol) and benzoyl isothiocyanate (0.171 g, 1.04 mmol) to afford the product (0.371 g); m.p. 219-222° C.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-bba5ca7fc6484a688e325bff451e122a
Source dataset
uspto-grants-2003_03
Patent number
US06528528B2

Reaction notes

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