HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzanilide → HCID 53941565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzanilide | HCID 84347 | — |
| Reactant | 3,5-Dichlorophenyl isothiocyanate | HCID 138776 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 53941565 | HCID 53941565 | 73% |
Reaction Steps
Prepared according to the procedure described for Example 60 using 3-aminobenzanilide (0.213 g, 1.0 mmol) and 3,5-dichlorophenyl isothiocyanate (0.208 g, 1.0 mmol). Trituration in ethyl acetate gave the product (0.304 g); m.p. 174-177° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-5814f930263b43bcbca0c5894f7ca440 |
| Source note | uspto-grants-2003_03 |