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HRID1859690

反应详情

EQUATION

反应方程式

HRID 1859690 的结构方程式

REACTANTS

反应物

2
结构：Nc1cccc(C(=O)Nc2ccccc2)c1
HCID84347

Benzamide, 3-amino-N-phenyl-

C13H12N2O

结构：S=C=Nc1cc(Cl)cc(Cl)c1
HCID138776

3,5-Dichlorophenyl isothiocyanate

C7H3Cl2NS

PRODUCTS

生成物

1
结构：O=C(Nc1ccccc1)c1cccc(NC(=S)Nc2cc(Cl)cc(Cl)c2)c1
HCID53941565

未命名化合物

收率 73%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Prepared according to the procedure described for Example 60 using 3-aminobenzanilide (0.213 g, 1.0 mmol) and 3,5-dichlorophenyl isothiocyanate (0.208 g, 1.0 mmol). Trituration in ethyl acetate gave the product (0.304 g); m.p. 174-177° C.

WORKUP

后处理

  1. customPrepared