3-Aminobenzanilide → HCID 53941565, compound

HRID 1859690Notes

Reaction equation

HRID 1859690 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][CH:16]=1)[C:5]([NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:6].[Cl:17][C:18]1[CH:19]=[C:20]([N:25]=[C:26]=[S:27])[CH:21]=[C:22]([Cl:24])[CH:23]=1>C(OCC)(=O)C>[Cl:17][C:18]1[CH:19]=[C:20]([NH:25][C:26](=[S:27])[NH:1][C:2]2[CH:3]=[C:4]([CH:14]=[CH:15][CH:16]=2)[C:5]([NH:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:6])[CH:21]=[C:22]([Cl:24])[CH:23]=1

Participants

4

Reactant 2

HCID 843473-AminobenzanilideHCID 1387763,5-Dichlorophenyl isothiocyanate

Product 1

HCID 53941565HCID 53941565, compoundYield 73%

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

Prepared according to the procedure described for Example 60 using 3-aminobenzanilide (0.213 g, 1.0 mmol) and 3,5-dichlorophenyl isothiocyanate (0.208 g, 1.0 mmol). Trituration in ethyl acetate gave the product (0.304 g); m.p. 174-177° C.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-5814f930263b43bcbca0c5894f7ca440
Source dataset
uspto-grants-2003_03
Patent number
US06528528B2

Reaction notes

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