HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorophenyl isothiocyanate → HCID 53815690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorophenyl isothiocyanate | HCID 138776 | — |
| Reactant | HCID 18626083 | HCID 18626083 | — |
| Product | HCID 53815690 | HCID 53815690 | 81.1% |
Reaction Steps
Prepared according to the procedure described for Example 78 using N-(3-amino-4-methoxyphenyl)-benzamide from Example 21 (0.88 g, 3.62 mmol) and 3,5-dichlorophenyl isothiocyanate (0.739 g, 3.62 mmol). Filtration without trituration afforded the product (1.31 g); m.p. 194-195° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-c9070dfc578b49ceb478ffbdeed70205 |
| Source note | uspto-grants-2003_03 |