HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-4-methoxybenzanilide → HCID 18626247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-4-methoxybenzanilide | HCID 8426 | — |
| Reactant | 2-Thiophenesulfonyl chloride | HCID 85518 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18626247 | HCID 18626247 | 89% |
Reaction Steps
Prepared according to the procedure described for Example 121 using 2-thiophenesulfonyl chloride (1.82 g, 10 mmol), 3-amino-4-methoxy-N-phenyl-benzamide (2.43 g, 10 mmol), and pyridine (25 mL) to afford the product (3.457 g); m.p. 180-183° C. after trituration in hexanes/ethyl acetate (1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528528B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-99e5a32a609245558ef4b04de6261ff1 |
| Source note | uspto-grants-2003_03 |