HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(4-benzyloxyphenyl)-2-phenoxypropionate → Ethyl 3-(4-hydroxyphenyl)-2-phenoxypropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(4-benzyloxyphenyl)-2-phenoxypropionate | HCID 18625773 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Ethyl 3-(4-hydroxyphenyl)-2-phenoxypropionate | HCID 18625748 | 63.2% |
Reaction Steps
In a similar manner to that described in Reference example 1(d), a reaction was carried out using ethyl 3-(4-benzyloxyphenyl)-2-phenoxypropionate (2.10 g), which is the product of Reference example 4(b) and palladium on carbon (5%, 0.32 g) and the reaction mixture was treated to afford the desired compound (1.01 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-6775c484f60d40c6a753d9aba90c1b03 |
| Source note | uspto-grants-2003_03 |