HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl methylmalonate → HCID 18625691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl methylmalonate | HCID 11857 | — |
| Reactant | (3-Bromopropyl)benzene | HCID 12503 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Product | HCID 18625691 | HCID 18625691 | 79.3% |
Reaction Steps
In a similar manner to that described in Reference example 2(a), a reaction was carried out using diethyl 2-methylmalonate (3.48 g), 3-phenylpropyl bromide (3.98 g) and sodium hydride (55% suspension in oil, 0.96 g) and the reaction mixture was treated to afford the desired compound (4.63 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-648244b233894a03849f93b1c2f85088 |
| Source note | uspto-grants-2003_03 |