HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 18625866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(2-Bromoethoxy)tetrahydro-2H-pyran | HCID 86621 | — |
| Reactant | HCID 18625714 | HCID 18625714 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 18625866 | HCID 18625866 | 80.2% |
Reaction Steps
In a similar manner to that described in Reference example 3(e), a reaction was carried out using ethyl 2-(4-hydroxybenzyl)-2-methyl-5-phenylvalerate (1.58 g), which is the product of Reference example 7(d), 2-(2-bromoethoxy)tetrahydropyran (0.94 g) and potassium carbonate (1.86 g) in dimethylacetamide and the reaction mixture was treated to afford the desired compound (1.64 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-d00c92a6152f4cffbb12f84b4794e06a |
| Source note | uspto-grants-2003_03 |