HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12134925, compound → Ethyl 3-(4-hydroxyphenyl)-2-methyl-2-phenoxypropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12134925 | HCID 12134925 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Ethyl 3-(4-hydroxyphenyl)-2-methyl-2-phenoxypropionate | HCID 11220314 | 100.7% |
Reaction Steps
In a similar manner to that described in Reference example 1(d), a reaction was carried out using ethyl 3-(4-benzyloxyphenyl)-2-methyl-2-phenoxypropionate (4.97 g), which is the product of Reference example 8(a), and palladium on carbon (5%, 0.75 g) and the reaction mixture was treated to afford the desired compound (3.85 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-d67f2987edf44b7ca13b021ec5256b3f |
| Source note | uspto-grants-2003_03 |