HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 18625731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(2-Bromoethoxy)tetrahydro-2H-pyran | HCID 86621 | — |
| Reactant | HCID 18626008 | HCID 18626008 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 18625731 | HCID 18625731 | 77.1% |
Reaction Steps
In a similar manner to that described in Reference example 3(e), a reaction was carried out using ethyl 3-(4-hydroxyphenyl)-2-(4-isopropylphenoxy)-2-methylpropionate (1.00 g), which is the product of Reference example 9(b), 2-(2-bromoethoxy)tetrahydropyran (1.84 g) and potassium carbonate (1.62 g) in dimethylacetamide and the reaction mixture was treated to afford the desired compound (1.06 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-bf1cb956fe5d4b73aecd88797835796b |
| Source note | uspto-grants-2003_03 |