HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 18625988, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 18625731 | HCID 18625731 | — |
| Product | HCID 18625988 | HCID 18625988 | 75.8% |
Reaction Steps
In a similar manner to that described in Reference example 3(t), a reaction was carried out using ethyl 2-(4-isopropylphenoxy)-2-methyl-3-[4-[2-(tetrahydropyran-2-yloxy)ethoxy]phenyl]propionate (1.06 g), which is the product of Reference example 9(c), and p-toluenesulfonic acid monohydrate (0.60 g) and the reaction mixture was treated to afford the desired compound (0.66 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-aff1438e42514b7e852d75bef456d839 |
| Source note | uspto-grants-2003_03 |