HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 3'-Methoxymethoxymethylbiphenyl-4-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 3'-methoxymethoxymethylbiphenyl-4-carboxylate | HCID 18625885 | — |
| Product | 3'-Methoxymethoxymethylbiphenyl-4-carboxylic acid | HCID 18626047 | 80.8% |
Reaction Steps
In a similar manner to that described in Example 2, a reaction was carried out using methyl 3′-methoxymethoxymethylbiphenyl-4-carboxylate (445 mg), which is the product of Reference example 15(b), and aqueous sodium hydroxide (1N, 3.10 ml) and the reaction mixture was treated to afford the desired compound (342 mg) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-40ff700d5bf94b92863678211224df37 |
| Source note | uspto-grants-2003_03 |