HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 4'-Methoxymethoxy-3',5'-dimethylbiphenyl-4-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 4'-methoxymethoxy-3',5'-dimethylbiphenyl-4-carboxylate | HCID 18625974 | — |
| Product | 4'-Methoxymethoxy-3',5'-dimethylbiphenyl-4-carboxylic acid | HCID 18625708 | 83.7% |
Reaction Steps
In a similar manner to that described in Example 2, a reaction was carried out using methyl 4′-methoxymethoxy-3′,5′-dimethylbiphenyl-4-carboxylate (1.24 g) and aqueous sodium hydroxide (1N, 8.20 ml) and the reaction mixture was treated to afford the desired compound (0.99 g) as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-eb415a7c1833460a88234ec39342e51a |
| Source note | uspto-grants-2003_03 |