HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 18625878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 18625937 | HCID 18625937 | — |
| Product | HCID 18625878 | HCID 18625878 | 87% |
Reaction Steps
In a similar manner to that described in Reference example 3(f), a reaction was carried out using ethyl 2-butyl-3-[4-[3-(tetrahydropyran-2-yloxy)propoxy]phenyl]propionate (4.42 g) and p-toluensulfonic acid monohydrate (2.57 g) and the reaction mixture was treated to afford the desired compound (3.02 g) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-72e36b6cf53043de95ec3bd90e162854 |
| Source note | uspto-grants-2003_03 |