HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(4-benzyloxyphenyl)-2-(4-methylphenoxy)propionate → Ethyl 3-(4-hydroxyphenyl)-2-(4-methylphenoxy)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(4-benzyloxyphenyl)-2-(4-methylphenoxy)propionate | HCID 18625971 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Ethyl 3-(4-hydroxyphenyl)-2-(4-methylphenoxy)propionate | HCID 18626029 | 103.9% |
Reaction Steps
In a similar manner to that described in Reference example 1(d), a reaction was carried out using ethyl 3-(4-benzyloxyphenyl)-2-(4-methylphenoxy)propionate (2.84 g), which is the product of Reference example 35(b), and palladium on carbon (284 mg) and the reaction mixture was treated to afford the desired compound (2.27 g) as a syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-4a4b0b236bc4468495f668469663b16c |
| Source note | uspto-grants-2003_03 |