HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 18625758, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 18626025 | HCID 18626025 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 18625758 | HCID 18625758 | 90.8% |
Reaction Steps
In a similar manner to that described in Reference example 37(b), a reaction was carried out using ethyl 3-(4-benzyloxyphenyl)-2-(4-trifluoromethoxyphenoxy)propionate (4.08 g), which is the product of Reference example 40(a), a solution of hydrogen bromide in acetic acid (25%, 40 ml) and potassium carbonate (1.68 g) and the reaction mixture was treated to afford the desired compound (2.98 g) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-4abd936878844e01b2409fe2b5c27cf0 |
| Source note | uspto-grants-2003_03 |