HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 18626038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 18625758 | HCID 18625758 | — |
| Reactant | tert-Butyl N-(2-((methylsulfonyl)oxy)ethyl)carbamate | HCID 22605302 | — |
| Product | HCID 18626038 | HCID 18626038 | 56.1% |
Reaction Steps
In a similar manner to that described in Reference example 25, a reaction was carried out using ethyl 3-(4-hydroxyphenyl)-2-(4-trifluoromethoxyphenoxy)propionate (2.93 g), t-butyl 2-methanesulfonyloxyethylcarbamate (4.73 g) and potassium carbonate (5.46 g) and the reaction mixture was treated to afford the title compound (2.28 g) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528525B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-e446d4740107464a8aee9342677ae222 |
| Source note | uspto-grants-2003_03 |