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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1860434Generated: October 30, 2026

Triethylamine → HCID 178443962, compound

https://huagongshe.com/reaction/1860434

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactant4-HeptanamineHCID 38665—
ReactantHCID 178425446HCID 178425446—
SolventEthyl AcetateHCID 8857—
ProductHCID 178443962HCID 178443962—

Reaction Steps

A mixture of compound (7) (730 mg, 2 mmol), 4-aminoheptane (250 mg, 2.2 mmol) and triethylamine (250 mg, 2.5 mmol) were stirred at ambient temperature for 16 hours. The solution was diluted with ethyl acetate and washed with brine. The organic layer was dried over sodium sulfate and evaporated to dryness to provide compound (8).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06531475B1
Source datasetuspto-grants-2003_03
ORD IDord-90aea66c5880495d84efb12c30174953
Source noteuspto-grants-2003_03