HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178443962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Heptanamine | HCID 38665 | — |
| Reactant | HCID 178425446 | HCID 178425446 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178443962 | HCID 178443962 | — |
Reaction Steps
A mixture of compound (7) (730 mg, 2 mmol), 4-aminoheptane (250 mg, 2.2 mmol) and triethylamine (250 mg, 2.5 mmol) were stirred at ambient temperature for 16 hours. The solution was diluted with ethyl acetate and washed with brine. The organic layer was dried over sodium sulfate and evaporated to dryness to provide compound (8).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06531475B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-90aea66c5880495d84efb12c30174953 |
| Source note | uspto-grants-2003_03 |