Benzoyl chloride, 3,4,5-trimethoxy- → HCID 461346, compound

Participants

Reaction Steps

Working again according to a protocol identical to the one used in step 1.3 of Example 1, followed by treating, under the same conditions as those of step 1.4 of Example 1, 0.5 g of 2-(1′-piperidinocarbonyloxymethyl)piperazine hydrochloride with 1.1 g of 3,4,5-trimethoxybenzoyl chloride, 0.8 g of 1,4-bis(3′,4′,5′-trimethoxybenzoyl)-2-(1′-piperidinocarbonyloxymethyl)piperazine is obtained. Yield: 56%. Melting point: 146.7° C.

Provenance & Evidence