Hydrochloric Acid → HCID 18623111, compound

HRID 1860471Notes

Reaction equation

HRID 1860471 reaction equation
Cl.C([N:4]1[CH2:9][CH2:8][N:7]([C:10]([NH:13][NH2:14])=[N:11][CH3:12])[CH2:6][CH2:5]1)=O>CO>[NH:13]([C:10](=[N:11][CH3:12])[N:7]1[CH2:6][CH2:5][NH:4][CH2:9][CH2:8]1)[NH2:14]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 23435349HCID 23435349, compound

Product 1

HCID 18623111HCID 18623111, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

10 g of the hydrochloride of 1-formyl-4-[hydrazino(methylimino)methyl]piperazine are dissolved in 250 ml of methanol. 50 ml of HClconc. are added, the mixture obtained is stirred overnight and the solvent is evaporated. A solid residue is obtained which is dried over solid KOH. The trihydrochloride of 1-[hydrazino(methylimino)methyl]piperazine is obtained in form of a white product.

Workup

  1. additionare added
  2. customthe mixture obtained
  3. customthe solvent is evaporated
  4. customA solid residue is obtained which
  5. dry with materialis dried over solid KOH

Sources & evidence

ORD record
ord-2af4489765af4f4a82b35e81bf943dda
Source dataset
uspto-grants-2003_03
Patent number
US06531465B1

Reaction notes

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