HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl 1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylate → HCID 9835275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl 1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylate | HCID 251472 | — |
| Reactant | HCID 21218215 | HCID 21218215 | — |
| Reactant | 6-(6-chloro-1-oxo-1,2,3,4-tetrahydro-naphthalen-2-yl)-hexanoic Acid Hydroxyamide | HCID 22977450 | — |
| Product | HCID 9835275 | HCID 9835275 | — |
Reaction Steps
6-(1-oxo-1,2,3,4-tetrahydro-naphthalen-2-yl)-hexanoic acid hydroxyamide (5a) is prepared from 1-oxo-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid ethyl ester (1a) in an analogous manner to that described for the conversion of 3a to 3c in example 3. Yield in the last step is 10%, MS (APCI): 274.1 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06531472B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-7dc7e151016c40f5848c436cfe25d342 |
| Source note | uspto-grants-2003_03 |