Sodium Hydroxide → HCID 18624194, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of the product of STEP 1 (45 g), ethanol (15 mL) and 15% aqueous NaOH (70 mL) was stirred at 23° C. for 30 minutes. The volatiles were removed in vacuo and the residue was acidified to pH=3. The precipitated solid was filtered and dried to give the above product as a white solid (40 g).

Provenance & Evidence