HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66919021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 66919000 | HCID 66919000 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 66919021 | HCID 66919021 | — |
Reaction Steps
Compound 3 (25 g) in 125 ml of THF was added with 63 ml of 1N LiOH at room temperature. After 30 minutes, the mixture was adjusted to a pH of 2 by adding 1N HCl. After separation of the aqueous part, the organic part was washed with brine and dried over MgSO4. Removing the solvent under reduced pressure gave quantitatively Compound 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06531611B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-7b7a12ad73a347afbcf019679f655749 |
| Source note | uspto-grants-2003_03 |