HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3,4-Trimethoxybenzaldehyde → 2,3-Bis-(2,3,4-trimethoxy-phenyl)-acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3,4-Trimethoxybenzaldehyde | HCID 75006 | — |
| Reactant | 2,3,4-Trimethoxyphenylacetonitrile | HCID 144317 | — |
| Product | 2,3-Bis-(2,3,4-trimethoxy-phenyl)-acrylonitrile | HCID 69779208 | 93.4% |
Reaction Steps
Following the Procedure A, the reaction was performed with 1.96 g of 2,3,4-trimethoxybenzaldehyde (10 mmol) and 2.07 g of 2,3,4-trimethoxyphenyl-acetonitrile (10 mmol), affording 2,3-bis-(2,3,4-trimethoxy-phenyl)-acrylonitrile as yellow powder (yield 3.6 g, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06534135B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-3ba7e9d8c2a149c0924e0fc391d31320 |
| Source note | uspto-grants-2003_03 |