2-Morpholinoethylamine → HCID 69988693, compound

Participants

Reaction Steps

Intermediate 3 (0.043 mg), 4-(2-aminoethyl)morpholine (0.053 mg), dimethyl sulphoxide (0.05 ml) ) in a sealed vial (eg Reactivial™) were heated at 90° C. for 16 hours. Purification by Autoprep HPLC afforded after freeze-drying the title compound as a pale yellow solid (0.019 g). LC-MS System A Rt=3.71 min, m/z 627 (MH+).

Provenance & Evidence