HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86758878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 9821409 | HCID 9821409 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86758878 | HCID 86758878 | — |
Reaction Steps
To a solution of 1-[2-(acetylthio) ethyl]-1-(2-cyclohexylethyl)-3-[2-(1-piperidyl) ethyl] urea (Compound 3-1, 618 mg) in ether, there was added a 4N hydrogen chloride solution in ethyl acetate (0.4 ml). The resulting precipitates were filtered off to give the title compound (Compound 6-1, 401 mg) in the form of crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06534499B2 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-38d774eace6e4f10b65c28fe1f8ef40d |
| Source note | uspto-grants-2003_03 |