Iodoethane → HCID 178477476, compound

HRID 1861902Notes

Reaction equation

HRID 1861902 reaction equation
[C:1]([O:5][C:6](=[O:19])[NH:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][C:16]([NH2:18])=[S:17])[CH:10]=1)([CH3:4])([CH3:3])[CH3:2].[CH2:20]([I:22])[CH3:21]>>[IH:22].[C:1]([O:5][C:6](=[O:19])[NH:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][C:16](=[NH:18])[S:17][CH2:20][CH3:21])[CH:10]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 18331431HCID 18331431, compound

Product 1

HCID 178477476HCID 178477476, compoundYield 68%

Procedure

Using the compound obtained in Example 24 as a starting material and also using ethyl iodide as a reagent, the same procedure of Example 4 gave 178 mg of the titled compound (yield, 68%).

Sources & evidence

ORD record
ord-2f7a0e634fa04e2a81756198a1ac35fe
Source dataset
uspto-grants-2003_03
Patent number
US06534546B1

Reaction notes

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