1-Iodopropane → HCID 178460858, compound

HRID 1861916Notes

Reaction equation

HRID 1861916 reaction equation
[C:1]([O:5][C:6](=[O:19])[NH:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][C:16]([NH2:18])=[S:17])[CH:10]=1)([CH3:4])([CH3:3])[CH3:2].[CH2:20](I)[CH2:21][CH3:22]>>[C:1]([O:5][C:6](=[O:19])[NH:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][C:16](=[NH:18])[S:17][CH2:20][CH2:21][CH3:22])[CH:10]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 336431-IodopropaneHCID 18331431HCID 18331431, compound

Product 1

HCID 178460858HCID 178460858, compoundYield 99%

Procedure

Using the compound obtained in Example 24 as a starting material and also using n-propyl iodide as a reagent, reaction was performed as in Example 29 to give 227 mg of the titled compound (yield, 99%).

Workup

  1. customreaction

Sources & evidence

ORD record
ord-e8c7e8fd82c04dc0903d2bea570353d1
Source dataset
uspto-grants-2003_03
Patent number
US06534546B1

Reaction notes

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