Butyl iodide → HCID 178454977, compound

HRID 1861917Notes

Reaction equation

HRID 1861917 reaction equation
[C:1]([O:5][C:6](=[O:19])[NH:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][C:16]([NH2:18])=[S:17])[CH:10]=1)([CH3:4])([CH3:3])[CH3:2].[CH2:20](I)[CH2:21][CH2:22][CH3:23]>>[C:1]([O:5][C:6](=[O:19])[NH:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][C:16](=[NH:18])[S:17][CH2:20][CH2:21][CH2:22][CH3:23])[CH:10]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 10962Butyl iodideHCID 18331431HCID 18331431, compound

Product 1

HCID 178454977HCID 178454977, compoundYield 92%

Procedure

Using the compound obtained in Example 24 as a starting material and also using n-butyl iodide as a reagent, reaction was performed as in Example 29 to give 220 mg of the titled compound (yield, 92%).

Workup

  1. customreaction

Sources & evidence

ORD record
ord-2684f8c765ea41a4a9d237c4ca11b0ca
Source dataset
uspto-grants-2003_03
Patent number
US06534546B1

Reaction notes

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