Iodoethane → HCID 178477472, compound

HRID 1861918Notes

Reaction equation

HRID 1861918 reaction equation
[C:1]([O:5][C:6](=[O:21])[NH:7][C:8]([CH3:20])([C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([NH:16][C:17]([NH2:19])=[S:18])[CH:11]=1)[CH3:9])([CH3:4])([CH3:3])[CH3:2].[CH2:22](I)[CH3:23]>>[C:1]([O:5][C:6](=[O:21])[NH:7][C:8]([CH3:9])([C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([NH:16][C:17](=[NH:19])[S:18][CH2:22][CH3:23])[CH:11]=1)[CH3:20])([CH3:2])([CH3:3])[CH3:4]

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 22981132N-(1-methyl-1-(3-thioureidophenyl)ethyl)carbamic acid t-butyl ester

Product 1

HCID 178477472HCID 178477472, compoundYield 97%

Procedure

Using the compound obtained in Example 3 as a starting material and also using ethyl iodide as a reagent, reaction was performed as in Example 29 to give 110 mg of the titled compound (yield, 97%).

Workup

  1. customreaction

Sources & evidence

ORD record
ord-74df4185f8da4ad19426042ee30f3f04
Source dataset
uspto-grants-2003_03
Patent number
US06534546B1

Reaction notes

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