HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-[2-(Dimethylamino)ethyl]aniline--hydrogen chloride (1/2)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | n,n-Dimethyl-2-(4-nitrophenyl)ethanamine | HCID 220557 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4-[2-(Dimethylamino)ethyl]aniline--hydrogen chloride (1/2) | HCID 53407838 | 85% |
Reaction Steps
Using the compound obtained in Example 97 as a starting material and after adding a solution of hydrogen chloride (4N) in 1,4-dioxane, the same procedure of Example 2 gave 2.37 g of the titled compound (yield, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06534546B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-70e02ef663034225aa2f79e8e43f9bb8 |
| Source note | uspto-grants-2003_03 |